Synthesis of 13C enriched sialyllactones and their characterization using isotope edited inverse detected NMR spectroscopy

Jacquelyn Gervay-Hague; Nellie N. Mamuya; Andrew R. Barber

doi:10.1016/S0040-4039(97)00237-2

Synthesis of ¹³C enriched sialyllactones and their characterization using isotope edited inverse detected NMR spectroscopy

Jacquelyn Gervay-Hague, Nellie N. Mamuya, Andrew R. Barber

Research output: Contribution to journal › Article › peer-review

6 Scopus citations

Abstract

¹³C enriched monosaccharide based sialyllactones were prepared in order to perform isotope edited NMR experiments for their characterization. In the inverse detected experiments only those protons long-range coupled to the enriched nuclei are detected, providing a potentially powerful tool for studying in vitro sialyllactone formation.

Original language	English (US)
Pages (from-to)	1865-1868
Number of pages	4
Journal	Tetrahedron Letters
Volume	38
Issue number	11
DOIs	https://doi.org/10.1016/S0040-4039(97)00237-2
State	Published - Mar 17 1997
Externally published	Yes

ASJC Scopus subject areas

Biochemistry
Organic Chemistry
Drug Discovery

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title = "Synthesis of 13C enriched sialyllactones and their characterization using isotope edited inverse detected NMR spectroscopy",

abstract = " 13C enriched monosaccharide based sialyllactones were prepared in order to perform isotope edited NMR experiments for their characterization. In the inverse detected experiments only those protons long-range coupled to the enriched nuclei are detected, providing a potentially powerful tool for studying in vitro sialyllactone formation.",

author = "Jacquelyn Gervay-Hague and Mamuya, {Nellie N.} and Barber, {Andrew R.}",

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AU - Mamuya, Nellie N.

AU - Barber, Andrew R.

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AB - 13C enriched monosaccharide based sialyllactones were prepared in order to perform isotope edited NMR experiments for their characterization. In the inverse detected experiments only those protons long-range coupled to the enriched nuclei are detected, providing a potentially powerful tool for studying in vitro sialyllactone formation.

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