Synthesis of 13C enriched sialyllactones and their characterization using isotope edited inverse detected NMR spectroscopy

Jacquelyn Gervay-Hague, Nellie N. Mamuya, Andrew R. Barber

Research output: Contribution to journal › Article

5 Citations (Scopus)

Abstract

13C enriched monosaccharide based sialyllactones were prepared in order to perform isotope edited NMR experiments for their characterization. In the inverse detected experiments only those protons long-range coupled to the enriched nuclei are detected, providing a potentially powerful tool for studying in vitro sialyllactone formation.

Original languageEnglish (US)
Pages (from-to)1865-1868
Number of pages4
JournalTetrahedron Letters
Volume38
Issue number11
DOIs
StatePublished - Mar 17 1997
Externally publishedYes

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Monosaccharides
Isotopes
Nuclear magnetic resonance spectroscopy
Protons
Magnetic Resonance Spectroscopy
Experiments
Nuclear magnetic resonance
In Vitro Techniques

ASJC Scopus subject areas

  • Biochemistry
  • Organic Chemistry
  • Drug Discovery

Cite this

Synthesis of 13C enriched sialyllactones and their characterization using isotope edited inverse detected NMR spectroscopy. / Gervay-Hague, Jacquelyn; Mamuya, Nellie N.; Barber, Andrew R.

In: Tetrahedron Letters, Vol. 38, No. 11, 17.03.1997, p. 1865-1868.

Research output: Contribution to journal › Article

Gervay-Hague, J, Mamuya, NN & Barber, AR 1997, 'Synthesis of 13C enriched sialyllactones and their characterization using isotope edited inverse detected NMR spectroscopy', Tetrahedron Letters, vol. 38, no. 11, pp. 1865-1868. https://doi.org/10.1016/S0040-4039(97)00237-2
Gervay-Hague J, Mamuya NN, Barber AR. Synthesis of 13C enriched sialyllactones and their characterization using isotope edited inverse detected NMR spectroscopy. Tetrahedron Letters. 1997 Mar 17;38(11):1865-1868. https://doi.org/10.1016/S0040-4039(97)00237-2
Gervay-Hague, Jacquelyn ; Mamuya, Nellie N. ; Barber, Andrew R. / Synthesis of 13C enriched sialyllactones and their characterization using isotope edited inverse detected NMR spectroscopy. In: Tetrahedron Letters. 1997 ; Vol. 38, No. 11. pp. 1865-1868.
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