Abstract
Acrylamidolactamine monomer were prepared in two steps using a modified procedure in a total 77% yield. The resulting monomer LAM were copolymerized with NIPAAm in presence of BisA as the crosslinking reagent using KPS/TMEDA as initiating system at 25°C. The polymer gels from various comonomer feed ratios were homogeneous and transparent. Swelling ratio measurement proved that the gels with less than 20 mol% LAM in feed showed temperature-responding behavior. DSC studies correlated well with the equilibrium SR studies.
| Original language | English (US) |
|---|---|
| Title of host publication | American Chemical Society, Polymer Preprints, Division of Polymer Chemistry |
| Editors | Anon |
| Publisher | ACS |
| Pages | 120-121 |
| Number of pages | 2 |
| Volume | 39 |
| Edition | 2 |
| State | Published - Aug 1998 |
| Event | Proceedings of the 1997 Boston Meeting - Boston, MA, USA Duration: Aug 23 1998 → Aug 27 1998 |
Other
| Other | Proceedings of the 1997 Boston Meeting |
|---|---|
| City | Boston, MA, USA |
| Period | 8/23/98 → 8/27/98 |
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ASJC Scopus subject areas
- Polymers and Plastics
Cite this
Synthesis of novel lactose-based hydrogels. / Zhou, W. J.; Hsieh, Y. L.; Kurth, M. J.; Krochta, J. M.
American Chemical Society, Polymer Preprints, Division of Polymer Chemistry. ed. / Anon. Vol. 39 2. ed. ACS, 1998. p. 120-121.Research output: Chapter in Book/Report/Conference proceeding › Conference contribution
}
TY - GEN
T1 - Synthesis of novel lactose-based hydrogels
AU - Zhou, W. J.
AU - Hsieh, Y. L.
AU - Kurth, M. J.
AU - Krochta, J. M.
PY - 1998/8
Y1 - 1998/8
N2 - Acrylamidolactamine monomer were prepared in two steps using a modified procedure in a total 77% yield. The resulting monomer LAM were copolymerized with NIPAAm in presence of BisA as the crosslinking reagent using KPS/TMEDA as initiating system at 25°C. The polymer gels from various comonomer feed ratios were homogeneous and transparent. Swelling ratio measurement proved that the gels with less than 20 mol% LAM in feed showed temperature-responding behavior. DSC studies correlated well with the equilibrium SR studies.
AB - Acrylamidolactamine monomer were prepared in two steps using a modified procedure in a total 77% yield. The resulting monomer LAM were copolymerized with NIPAAm in presence of BisA as the crosslinking reagent using KPS/TMEDA as initiating system at 25°C. The polymer gels from various comonomer feed ratios were homogeneous and transparent. Swelling ratio measurement proved that the gels with less than 20 mol% LAM in feed showed temperature-responding behavior. DSC studies correlated well with the equilibrium SR studies.
UR - http://www.scopus.com/inward/record.url?scp=0032141221&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=0032141221&partnerID=8YFLogxK
M3 - Conference contribution
VL - 39
SP - 120
EP - 121
BT - American Chemical Society, Polymer Preprints, Division of Polymer Chemistry
A2 - Anon, null
PB - ACS
ER -