Synthesis of novel lactose-based hydrogels

W. J. Zhou; Y. L. Hsieh; M. J. Kurth; J. M. Krochta

Synthesis of novel lactose-based hydrogels

W. J. Zhou, Y. L. Hsieh, M. J. Kurth, J. M. Krochta

Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

Acrylamidolactamine monomer were prepared in two steps using a modified procedure in a total 77% yield. The resulting monomer LAM were copolymerized with NIPAAm in presence of BisA as the crosslinking reagent using KPS/TMEDA as initiating system at 25°C. The polymer gels from various comonomer feed ratios were homogeneous and transparent. Swelling ratio measurement proved that the gels with less than 20 mol% LAM in feed showed temperature-responding behavior. DSC studies correlated well with the equilibrium SR studies.

Original language	English (US)
Title of host publication	American Chemical Society, Polymer Preprints, Division of Polymer Chemistry
Editors	Anon
Publisher	ACS
Pages	120-121
Number of pages	2
Volume	39
Edition	2
State	Published - Aug 1998
Event	Proceedings of the 1997 Boston Meeting - Boston, MA, USA Duration: Aug 23 1998 → Aug 27 1998

Other

Other	Proceedings of the 1997 Boston Meeting
City	Boston, MA, USA
Period	8/23/98 → 8/27/98

ASJC Scopus subject areas

Polymers and Plastics

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title = "Synthesis of novel lactose-based hydrogels",

abstract = "Acrylamidolactamine monomer were prepared in two steps using a modified procedure in a total 77% yield. The resulting monomer LAM were copolymerized with NIPAAm in presence of BisA as the crosslinking reagent using KPS/TMEDA as initiating system at 25°C. The polymer gels from various comonomer feed ratios were homogeneous and transparent. Swelling ratio measurement proved that the gels with less than 20 mol% LAM in feed showed temperature-responding behavior. DSC studies correlated well with the equilibrium SR studies.",

author = "Zhou, {W. J.} and Hsieh, {Y. L.} and Kurth, {M. J.} and Krochta, {J. M.}",

year = "1998",

month = aug,

language = "English (US)",

volume = "39",

pages = "120--121",

editor = "Anon",

booktitle = "American Chemical Society, Polymer Preprints, Division of Polymer Chemistry",

publisher = "ACS",

edition = "2",

note = "Proceedings of the 1997 Boston Meeting ; Conference date: 23-08-1998 Through 27-08-1998",

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T1 - Synthesis of novel lactose-based hydrogels

AU - Zhou, W. J.

AU - Hsieh, Y. L.

AU - Kurth, M. J.

AU - Krochta, J. M.

PY - 1998/8

Y1 - 1998/8

N2 - Acrylamidolactamine monomer were prepared in two steps using a modified procedure in a total 77% yield. The resulting monomer LAM were copolymerized with NIPAAm in presence of BisA as the crosslinking reagent using KPS/TMEDA as initiating system at 25°C. The polymer gels from various comonomer feed ratios were homogeneous and transparent. Swelling ratio measurement proved that the gels with less than 20 mol% LAM in feed showed temperature-responding behavior. DSC studies correlated well with the equilibrium SR studies.

AB - Acrylamidolactamine monomer were prepared in two steps using a modified procedure in a total 77% yield. The resulting monomer LAM were copolymerized with NIPAAm in presence of BisA as the crosslinking reagent using KPS/TMEDA as initiating system at 25°C. The polymer gels from various comonomer feed ratios were homogeneous and transparent. Swelling ratio measurement proved that the gels with less than 20 mol% LAM in feed showed temperature-responding behavior. DSC studies correlated well with the equilibrium SR studies.

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UR - http://www.scopus.com/inward/citedby.url?scp=0032141221&partnerID=8YFLogxK

M3 - Conference contribution

AN - SCOPUS:0032141221

VL - 39

SP - 120

EP - 121

BT - American Chemical Society, Polymer Preprints, Division of Polymer Chemistry

A2 - Anon, null

PB - ACS

T2 - Proceedings of the 1997 Boston Meeting

Y2 - 23 August 1998 through 27 August 1998

ER -