Microwave assisting solid phase organic reaction monitored by FTIR

Aiming Yu, Zheng Pu Zhang, Hua Zheng Yang, Chun Xiang Zhang, Zhun Liu

Research output: Contribution to journalArticle

Abstract

Microwave assisting the addition reaction of Wang resin bound secondary amine 1 and isocyanate was carried out for the first time. The reaction time course was determined by analyzing FTIR spectra obtained using the improved KBr pellet method by grinding down the resin beads prior to recording. The results showed that the reaction assisted by microwave was accomplished only in 12 min, while the reaction without microwave was completed in 210 min.

Original languageEnglish (US)
JournalKao Teng Hsueh Hsiao Hua Heush Hsueh Pao/ Chemical Journal of Chinese Universities
Volume19
Issue number10
StatePublished - 1998
Externally publishedYes

Keywords

  • FTIR
  • Microwave irradiation
  • Resin beads
  • Solid phase organic reaction

ASJC Scopus subject areas

  • Chemistry(all)

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