Electrochemical synthesis and characterization of NaCuO 2

Gerald L. Roberts, Susan M. Kauzlarich

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

NaCuO 2 has been prepared via electrodeposition from a sodium hydroxide/potassium hydroxide melt and characterized by single crystal and powder X-ray diffraction, magnetic susceptibility, and resistivity. Clusters of blue-black plate-like and needle crystals are grown at positive potentials on a platinum anode with a platinum or a zirconium crucible serving as the cathode and a platinum reference electrode. Details of the electrochemical procedure are described, along with a cyclic voltammogram. NaCuO 2 exhibits temperature independent paramagnetism over the temperature range 30 - 300 K. Its room temperature resistivity is greater than 10 6 Ω-cm.

Original languageEnglish (US)
Title of host publicationMaterials Research Society Symposium - Proceedings
PublisherMaterials Research Society
Pages457-461
Number of pages5
Volume346
StatePublished - 1994
EventProceedings of the 1994 MRS Spring Meeting - San Francisco, CA, USA
Duration: Apr 4 1994Apr 8 1994

Other

OtherProceedings of the 1994 MRS Spring Meeting
CitySan Francisco, CA, USA
Period4/4/944/8/94

Fingerprint

Platinum
Paramagnetism
Potassium hydroxide
Sodium Hydroxide
Crucibles
Magnetic susceptibility
Zirconium
Electrodeposition
Needles
X ray powder diffraction
Temperature
Anodes
Cathodes
Sodium
Single crystals
Crystals
Electrodes

ASJC Scopus subject areas

  • Electronic, Optical and Magnetic Materials

Cite this

Roberts, G. L., & Kauzlarich, S. M. (1994). Electrochemical synthesis and characterization of NaCuO 2 In Materials Research Society Symposium - Proceedings (Vol. 346, pp. 457-461). Materials Research Society.

Electrochemical synthesis and characterization of NaCuO 2 . / Roberts, Gerald L.; Kauzlarich, Susan M.

Materials Research Society Symposium - Proceedings. Vol. 346 Materials Research Society, 1994. p. 457-461.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Roberts, GL & Kauzlarich, SM 1994, Electrochemical synthesis and characterization of NaCuO 2 in Materials Research Society Symposium - Proceedings. vol. 346, Materials Research Society, pp. 457-461, Proceedings of the 1994 MRS Spring Meeting, San Francisco, CA, USA, 4/4/94.
Roberts GL, Kauzlarich SM. Electrochemical synthesis and characterization of NaCuO 2 In Materials Research Society Symposium - Proceedings. Vol. 346. Materials Research Society. 1994. p. 457-461
Roberts, Gerald L. ; Kauzlarich, Susan M. / Electrochemical synthesis and characterization of NaCuO 2 Materials Research Society Symposium - Proceedings. Vol. 346 Materials Research Society, 1994. pp. 457-461
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